ASTM D6501-2004 卤水中磷酸盐的标准试验方法

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【英文标准名称】:StandardTestMethodforPhosphonateinBrines
【原文标准名称】:卤水中磷酸盐的标准试验方法
【标准号】:ASTMD6501-2004
【标准状态】:现行
【国别】:
【发布日期】:2004
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:D19.05
【标准类型】:(TestMethod)
【标准水平】:()
【中文主题词】:试验方法;磷;分析;含盐废水;磷酸盐;比色的
【英文主题词】:analysis;brine;colorimetric;phosphonate;scaleinhibitor
【摘要】:Thistestmethodisusefulforthedeterminationoftracelevelphosphonateresiduesinbrines.Chemicaltreatmentwhichcontainphosphonatesareusedasmineralscaleandcorrosioninhibitorsingasandoildrillingandproductionoperations;andotherindustrialapplications.Often,thedecisionfortreatmentisbasedontheabilitytomeasurelowphosphonateconcentrationandnotuponperformancecriteria.Phosphonateconcentrationsaslowas0.16mg/Lhavebeenshowneffectiveincarbonatescaletreatment.Thistestmethodenablesthemeasurementofsub-mg/Lphosphonateconcentrationinbrinescontaininginterferingelements.Theprocedureincludesmeasuringtotal(see12.3.8)andfreeorthophosphate(see12.4.3)ionsandthedifferenceinconcentrationisthephosphonateconcentration.Thesamplecouldcontainorthophosphatenaturally,orfromdecompositionofthephosphonateduringprocessingorwelltreatmentorfromtreatingcompoundscontainingmoleculardehydratedphosphates.1.1Thistestmethodcoversthecolorimetricdeterminationofphosphonate(PNA)inbrinesfromgasandoilproductionoperationsintherangefrom0.1to5mg/L.1.2Thisphosphonatemethodisintendedforusetoanalyzelowconcentrationofphosphonateinbrinecontaininginterferingelements.Thistestmethodismostusefulforanalyzingphosphonateat0.1to1mg/Lrangeinbrineswithinterferingelements;however,itrequirespersonnelwithgoodanalyticalskill.1.3Thistestmethodhasbeenusedsuccessfullywithreagentwaterandbothfieldandsyntheticbrine.Itistheuser'sresponsibilitytoensurethevalidityofthistestmethodforwatersofuntestedmatrices.1.4Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.Forspecifichazardstatements,see9.1.3.
【中国标准分类号】:G12
【国际标准分类号】:75_020
【页数】:10P.;A4
【正文语种】: